purification scandium recovery

Radiochemical purification of no-carrier-added scandium-47 ...

Results of this comparison led to the development of an optimized procedure based on cation-exchange with Dowex AG 50W-X4 and 47Sc elution with HCl/HF. This method gave 90-97% overall 47Sc recovery, with a Ti separation factor greater than 2.4 x 10( …

Overview of the Purification of Recombinant Proteins

One of the main purposes of constructing fusion proteins is to facilitate the recovery and purification of the recombinant protein. The most popular fusion partners are the poly-histidine tag (His-tag) and the glutathione-S-transferase (GST-tag), these are discussed in more detail in UNITS 6.5 & 6.6.

Recovery of scandium from synthetic red mud leach ...

Apr 19, 2013· The extraction of scandium from an Australian red mud by selective acid leaching has been explored and the recovery of scandium from a synthetic leach solution using solvent extraction studied. Preliminary leaching tests showed that H 2 SO 4 performed best with highest scandium leaching efficiency amongst the three mineral acids tested.

Research on Scandium Recovery and Extraction Process ...

[10] Wang W W, Cheng C Y. Separation and purification of scandium by solvent extraction and related technologies: a review[J]. Journal of Chemical Technology and Biotechnology, 2011, 86(10): 1237. DOI: 10.1002/jctb.2655

US4968504A - Recovery of scandium and uranium - Google Patents

The separation of uranium, iron and scandium is achieved by the following process wherein a material containing these values is dissolved in mineral acid to form an aqueous solution, thereafter, an iminodiacetic acid cationic ion exchange resin is used to retain a major portion of the scandium and uranium. A raffinate containing the iron is formed.

Ion exchange method for the purification of scandium - GTE ...

The scandium is precipated from the ammonium nitrate by adding oxalic acid. The precipate of scandium oxalate is collected by filtration and rinsed. The precipate is calcined at approximately 975° C. to form scandium oxide. This process is applicable to the recovery and purification of scandium from any acid soluble matrix.

US5019362A - Ion exchange method for the purification of ...

(PDF) Recovery of scandium from magnesium, aluminium and ...

[15] Thus it urges the further purification for selective recovery of scandium from the above leach liquor. Though, there have been ample of studies for recovery of Sc form various sources with ...

Recovery of scandium from sulfation-roasted leachates of ...

Apr 04, 2017· Recovery and purification of scandium from the obtained leachates is generally performed using either solvent extraction or ion-exchange chromatography, or a combination of the two techniques,,,,,,, .

Ion exchange purification of scandium (Patent) | DOE Patents

Oct 23, 1990· Recovery of scandium is improved by pumping dilute scandium over the column prior to stripping the scandium and precipitation. This eliminates the HEDTA ion and other monovalent cations contaminating the scandium band. This method maximizes recovery of scandium while maintaining purity. 2 figs. ... {Ion exchange purification of scandium ...

Recovery of Scandium(III) from Aqueous Solutions by ...

Extraction of Scandium (Sc) Using a Task-Specific Ionic Liquid Protonated Betaine Bis(Trifluoromethylsulfonyl)Imide [Hbet][Tf2N]. 2018,,, 2723-2734. DOI: 10.1007/978-3-319-95022-8_230. Zhaobo Liu, Hongxu Li, Qiankun Jing, Mingming Zhang. Recovery of Scandium from Leachate of Sulfation-Roasted Bayer Red Mud by Liquid–Liquid Extraction.

Highly efficient recovery and purification of scandium ...

The waste sulfuric acid solution generated from titanium dioxide production is called titanium dioxide waste acid (TWWA), which is an important resource for scandium production. A way including enrichment and purification stages for recovery and purification of Sc from TWWA with 10% P204 - 5% TBP synergistic extraction system was studied.

Recovery of Scandium by Crystallization Techniques ...

Jan 25, 2019· The current state-of-the-art in the recovery of scandium from metallurgical waste streams involves leaching to extract scandium from the waste stream, e.g., bauxite residue [13,14,15]. Solvent extraction is then employed to extract Sc from the pregnant leach solution (PLS) using an organic solvent, followed by stripping of Sc back into the ...

Separation and purification of scandium by solvent ...

May 27, 2011· Scandium(III) extractions are interfered with by commonly associated elements such as iron(III), zirconium(IV), titanium(IV), thorium(IV), yttrium(III) and lanthanides(III). The advantages and disadvantages of applications of ion exchange and liquid membrane technologies for scandium recovery are reviewed and compared with solvent extraction.

US4965053A - Ion exchange purification of scandium ...

This method maximizes recovery of scandium while maintaining purity. An improvement in purification of scandium through ion exchange chromatography is disclosed in which the oxidation potential of the eluting solution is altered by the addition of potassium chlorate or ammonium chloride so that removal of contaminants is encouraged.

First Production of High Purity (99.9%) Scandium Oxide at ...

The demonstration plant simulated the Scandium recovery and purification process to be used at Clean TeQ's owned Syerston Project in NSW. During September and October, the demonstration plant campaign, which included commissioning and operation of the entire leaching and extraction circuit,

US10570480B2 - Method for recovering scandium - Google Patents

The invention provides a method for recovering scandium from an acidic solution containing scandium. The method having [a] a precipitation step wherein sodium sulfate is added into the acidic solution containing scandium to obtain a precipitate of a scandium double sulfate; [b] a neutralization step wherein pure water is added to the precipitate of a scandium double sulfate to dissolve the ...

Recovery of scandium from synthetic red mud leach ...

The extraction of scandium from an Australian red mud by selective acid leaching was explored and preliminary leaching tests showed that diluted sulphuric acid can be used to leach scandium from the red mud. The recovery of scandium from a synthetic leach …

WO2016151959A1 - Method for recovering scandium - …

Provided is a method for recovering scandium, which enables easy and efficient recovery of high-quality scandium from an acidic solution containing scandium. According to this method for recovering scandium, an acidic solution containing scandium is used and a scandium dissolution liquid after purification is obtained by a double sulfate precipitation step including the steps [A]-[C] described ...

Microblog: Scandium, Cobalt, and Water Purification ...

Cobalt has a similar supply situation as scandium, it is mostly a by-product and is not commonly a prime mining target in and of itself. But demand for the electric energy market is growing rapidly and cobalt demand is growing and will continue to grow accordingly. Supply chains on cobalt are iffy. (3) Water purification is a pressing need ...

Recovery of scandium from bauxite residue—red mud: a ...

Oct 21, 2016· Wang W, Cheng CY. Separation and purification of scandium by solvent extraction and related technologies: a review. J Chem Technol Biotechnol. 2011;86(10):1237. Article Google Scholar [97] Zhang J, Deng Z, Xu T. Recovery scandium from leaching liquor of red mud. Light Met. 2006;7:16. Google Scholar [98]

Scandium recovery from ion-adsorption rare earth ...

Apr 13, 2021· An excellent extraction selectivity towards Sc over other REEs in 4 mol/L HCl solution was achieved with the separation factor βSc/REEs over 8000 by 2-ethylhexyl phosphoric acid mono 2-ethylhexyl ester (HEHEHP) and the extraction equilibrium can be obtained within 20 min. The extracted Sc can be stripped using 5 mol/L NaOH solution as eluent at 363 K with the stripping rate of 92.1% …

Ion exchange purification of scandium (Patent) | DOE Patents

Oct 23, 1990· Recovery of scandium is improved by pumping dilute scandium over the column prior to stripping the scandium and precipitation. ..., abstractNote = {An improvement in purification of scandium through ion exchange chromatography is disclosed in which the oxidation potential of the eluting solution is altered by the addition of potassium chlorate ...

JP5403115B2 - Scandium separation and purification method ...

scandium extraction solution organic solvent extracted Prior art date Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.) Active Application number JP2012137891A Other languages Japanese (ja ...

Selective recovery of vanadium and scandium by ion ...

Selective recovery of vanadium and scandium by ion exchange with D201 and solvent extraction using P507 from hydrochloric acid leaching solution of red mud Chemosphere . 2017 May;175:365-372. doi: 10.1016/j.chemosphere.2017.02.083.

Efficient and Selective Recovery of Trace Scandium by ...

Mar 02, 2017· Bauxite residue (BR) is an inevitable industrial waste generated through the classic Bayer extraction of alumina from bauxite minerals. It contains relatively significant amount of valuable rare earth elements, including scandium, and therefore, we explored the suitability of trace scandium recovery from BR acid leachate by titanium phosphate (TiP) ion exchangers.

Highly efficient recovery and purification of scandium ...

Aug 01, 2021· Request PDF | Highly efficient recovery and purification of scandium from the waste sulfuric acid solution from titanium dioxide production by solvent extraction | …

Scandium Solvent Extraction & Purification – Core Group

> Scandium Solvent Extraction & Purification In 2011-2012, Core carried out a series of batch and pilot plant programmes to test and optimise a new solvent extraction (SX) technology for Scandium. Generating 1000 g of Ultrapure Scandium Oxide

Scandium recovery method - SUMITOMO METAL MINING CO., …

separation and purification method of scandium: jp2014012901a: : separation and purification method of scandium: jp2014218719a: : scandium collecting method: jp2015163729a: : scandium recovery method: wo2012014685a1: : process for production of ferronickel smelting raw material from low grade lateritic ...

(PDF) Recovery of Rare Earth Elements and Scandium from ...

Scandium purification will follow using a separate flowsheet. ... recovery of the Scandium content in bauxite r esidues (red mud), em anating from primar y aluminium . production in Greece.

(PDF) Accepted Manuscript Recovery of scandium from ...

Recovery of scandium from synthetic red mud leach solutions by solvent extraction with D2EHPA Weiwei Wang, Yoko Pranolo and Chu Yong Cheng* Parker Centre / CSIRO Process Science and Engineering CSIRO Minerals Down Under National Research Flagship 7 Conlon Street, Waterford, WA 6152, Australia *Corresponding author email: [email protected] ...

Research on Scandium Recovery and Extraction Process

The feasibility of selective recovery of titanium and scandium from a high acidic content lixivium by solvent extraction was verified in this study.

Imperial Mining Develops High-Recovery Extraction Process

Jun 09, 2021· The method showed scandium recovery to primary leach solution (PLS) of 87% for MET01, and 84% for MET02 samples. The recovery of total rare earth element, including yttrium (TREE+Y) of 84%, from ...

Why Scandium Solvent Extraction Is Better Than Traditional ...

If there are significant amounts of uranium, thorium and rare earths in the ore body being leached, these can be concentrated up along with the scandium, requiring a secondary purification step. Scandium Recovery Using D2EHPA. The use of D2EHPA (di-2-ethylhexyl phosphoric acid) for recovery of scandium from solution has been known for many years.

Separation and purification of scandium by solvent ...

Oct 01, 2011· Separation and purification of scandium by solvent extraction and related technologies: a review Wang, Weiwei; Cheng, Chu Yong 00:00:00 INTRODUCTION Scandium is a rare element, and is a very expensive metal due to its scarcity and to the rather complicated metallurgical processes for its purification and recovery. In 2009, the price ...

purification scandium recovery

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